ASTM D Standard Recommended Practice for Preparation of Metal. Surfaces for Adhesive Bonding. ASTM D Standard Guide for. D – Designation: D – 98 AMERICAN SOCIETY FOR TESTING PA Reprinted from the Annual Book of ASTM Standards. D, Method r, and ASTM E involves the etching of aluminum dure is described in ASTM D and involves the application of.

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It is recommended for screening durability of surface preparation-primer-adhesive systems through the analysis of crack growth and mode and locus of joint failure.

Phosphoric acid anodizing is porous and provides a substrate for mechanical locking, so I suppose that is why you need it for the adhesion test. The methods may be revised or supplemented, as necessary, to include methods based on proven performance.

I am not an aircraft engineer and cannot give you an authoritative answer; but maybe this help you until someone more knowledgable steps forward. I don’t think dd3933 is possible, but I thought I should at least try to post the question.

I am trying out Phosphoric Acid anodizing for a new customer. My basic question is: We have been told that the sulfuric acid 3d933 is more temperature sensitive, and we might have to install a chiller and a heat exchanger to control the temperature. Phosphoric acid anodizing is porous and provides a substrate for mechanical locking, so I suppose that is why you need it for the adhesion test.

Standard Guides for Automotive and Aerospace Adhesives from ASTM

This standard is subject to revision at any time by the responsible technical committee and must be reviewed every? Chromate can withstand and in some cases mostly material dependent I have seen in cases it pass hours. The method may be revised or supplemented, as necessary, to include methods based on proven performance. Need more than one copy? Need more than one copy? This standard is also available to be included in Standards Subscriptions.


I would suggest starting there with some of the engineering requirements then go to the PAA spec. For alloys with a lot of Chrome, the solution will become a greenish color. Is there any literature about the advantages and problems associated with switching from phosphoric acid to sulfuric acid anodizing? You can download and open this file to your own computer but DRM prevents opening this file on another computer, including a networked server.

The values given in parentheses are for information only. Standards Subsctiption may be the perfect solution.

Phosphoric Acid Anodizing (PAA Process, primarily for adhesive bonding of aluminum)

There is even a standard related to adhesive odor: Anodize at ASF for minutes. See D [link by ed. In theory, his invention x3933 a potential fit in other applications, but he targeted automotive as his first foray to solve a vexing industry problem.

Use the following formula: We previously had not experienced this yellow color change until we recently improved the electrical contacts and the mechanical contacts holding the parts to the racks. The next best process to PAA would be any method of etching the aluminum surface to roughen the profile.

I have searched the web and cannot find much technical info. James’ recommendation was fromand even then the e3933 Metals Finishing Process Manual” was quite hard to find.


This guide describes the requirements for phosphoric acid anodizing of aluminum and its alloys for structural adhesive bonding.

Asttm you see an affordable copy anywhere these days, grab it: The Mil spec was written to get people to use stressed, environmental testing for adhesive bonding quality control instead of relying only on plain lap shear tests and to use good overall practices. Equally important, the data had to be easily verifiable, and his proven methodology had to be universally accepted for verifying the required adhesive bonding properties.

Please first verify your email before subscribing to alerts. There are very stringent requirements for application and inspection of phosphoric acid anodized aetm [for aerospace application]. Other considerations include temperature and humidity effects on joint strength, moisture inhibitors, and retaining joint integrity in cyclic environmental conditions. One option was to eliminate the entire process aetm propose Asttm Beam Assisted Deposition treatment to the components.

I was hoping someone could suggest a filtration technique for the acid tanks to keep chloride and fluoride levels down to acceptable levels 35 ppm for chloride, 75 ppm for fluoride. The specification for the adhesion test should have the parameters you need for applying the anodic coating.

First of all, you probably want to use stainless steel cathodes instead of aluminum for PAA.